HCID 86617469, compound → HCID 86617468, compound

Participants

Reaction Steps

To 54 mg (0.12 mmol) of the product from Step A in 4 mL of methanol was added 10 mg of 20% palladium hydroxide on carbon. The reaction mixture was purged with hydrogen gas and held under 1 atmosphere of hydrogen for 2 h. The mixture was filtered through a pad of Celite, and the filter cake was successively washed with three portions of methanol. The combined filtrate and washings were concentrated and used without further purification. LC/MS 433.1 (M+1).

Provenance & Evidence