HRID2239203

反应详情

EQUATION

反应方程式

HRID 2239203 的结构方程式

PROCEDURE

实验过程

Paraformaldehyde was added to 4-oxo-2-hydroxyadamantane, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this 4-oxo-2-hydroxyadamantane. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 4-oxo-2-adamantyl chloromethyl ether (compound 1) represented by the following chemical formula (58).

WORKUP

后处理

  1. customAfter the completion of the reaction