HCID 53943327, compound → HCID 67243612, compound

HRID 2239604Notes

Reaction equation

HRID 2239604 reaction equation
C(OC([NH:8][CH2:9][CH2:10][C:11]([O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[O:12])=O)(C)(C)C.[ClH:20].NCCCC(OC1C(C)=CC=CC=1C)=O>>[ClH:20].[NH2:8][CH2:9][CH2:10][C:11]([O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[O:12]

Participants

3

Reactant 2

HCID 53943327HCID 53943327, compoundHCID 67242907HCID 67242907, compound

Product 1

HCID 67243612HCID 67243612, compound

Procedure

The title compound was prepared from phenyl N-(tert-butoxycarbonyl)-β-alaninate in a similar manner as described for 2,6-dimethylphenyl 4-aminobutanoate hydrochloride. 1H NMR (400 MHz, CDCl3): δ 7.36-7.40 (t, 2H), 7.22-7.25 (t, 1H), 7.12-7.14 (d, 2H), 4.82 (s, 3H), 3.27-3.30 (m, 2H), 2.99-3.03 (t, 2H).

Sources & evidence

ORD record
ord-47fe98c4784146ef85d98c4d6ef72d40
Source dataset
uspto-grants-2010_05
Patent number
US07723333B2

Reaction notes

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