HCID 59128266, compound → HCID 178483161, compound

HRID 2240095Notes

Reaction equation

HRID 2240095 reaction equation
[CH3:1][N:2]([CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([N+:15]([O-])=O)=[C:11]([CH2:18][S:19]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)(=[O:21])=[O:20])[CH:10]=1)C(=O)OC.C[N:29](CCC1C=CC([N+]([O-])=O)=CC=1)C(=O)OC>>[CH3:1][NH:2][CH2:7][CH2:8][C:9]1[CH:10]=[C:11]2[C:12](=[CH:13][CH:14]=1)[NH:15][N:29]=[C:18]2[S:19]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)(=[O:21])=[O:20]

Participants

3

Reactant 2

HCID 59128266HCID 59128266, compoundHCID 59128268HCID 59128268, compound

Product 1

HCID 178483161HCID 178483161, compound

Procedure

Methyl methyl(2-{4-nitro-3-[(phenylsulfonyl)methyl]phenyl}ethyl)carbamate Using substantially the same manner as described in Example 171, step 1 and employing methyl methyl[2-(4-nitrophenyl)ethyl]carbamate (2.47 g, 10.38 mmol), the title compound was obtained as a white solid, (2.06 g, 51%). Mp: 42° C., MS (ES+): 393 (M+H)+. Step 4

Sources & evidence

ORD record
ord-c8a2441fce9b4a089be7a08a4b8a046f
Source dataset
uspto-grants-2010_05
Patent number
US07723329B2

Reaction notes

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