Aluminium lithium hydride → HCID 68584177, compound

HRID 2240383Notes

Reaction equation

HRID 2240383 reaction equation
[F:1][C:2]1[CH:12]=[CH:11][C:5]([C:6](OCC)=[O:7])=[CH:4][C:3]=1[O:13][C:14]1[CH:19]=[N:18][CH:17]=[CH:16][N:15]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[F:1][C:2]1[CH:12]=[CH:11][C:5]([CH2:6][OH:7])=[CH:4][C:3]=1[O:13][C:14]1[CH:19]=[N:18][CH:17]=[CH:16][N:15]=1

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 68583578HCID 68583578, compound

Product 1

HCID 68584177HCID 68584177, compound

Procedure

The product of Example 128B and LiAlH4 were processed according to the method of Example 124B to provide the product. MS (ESI+) m/z 221 (M+H)+.

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-f498a4ecd738443cbbd3b5a252cdc898
Source dataset
uspto-grants-2010_05
Patent number
US07723367B2

Reaction notes

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