HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2240983Generated: October 30, 2026
3-Bromobenzaldehyde → HCID 67538669, compound
https://huagongshe.com/reaction/2240983
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Bromobenzaldehyde | HCID 76583 | — |
| Reactant | HCID 178476833 | HCID 178476833 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Product | HCID 67538669 | HCID 67538669 | 98.3% |
Reaction Steps
Into a mixture of 3-bromobenzaldehyde (20 g, 108.1 mmol) and diethyl phosphonate (14.2 g, 108.1 mmol) was added triethylamine (0.44 g, 4.32 mmol) and the mixture was stirred at 40° C. for 72 hours. Purification by ISCO (hexane/EtOAc 1/1) gave diethyl[(3-bromophenyl)(hydroxy)methyl]phosphonite (32.62 g); MS m/e (M)+ 322.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07723368B2 |
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| Source dataset | uspto-grants-2010_05 |
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| ORD ID | ord-83010bd766dc4bbfabff2d2fa224e08c |
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| Source note | uspto-grants-2010_05 |
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