HCID 24780800, compound → HCID 24780802, compound

HRID 2241819Notes

Reaction equation

HRID 2241819 reaction equation
[F:1][CH2:2][CH2:3][N:4]([C:12]1[N:17]=[CH:16][C:15]([C:18]2[O:19][C:20]3[CH:26]=[C:25]([O:27][CH3:28])[CH:24]=[CH:23][C:21]=3[N:22]=2)=[CH:14][N:13]=1)C(=O)OC(C)(C)C.FCCNC1C=CC(C2OC3C=C(OC)C=CC=3N=2)=CN=1>>[F:1][CH2:2][CH2:3][NH:4][C:12]1[N:13]=[CH:14][C:15]([C:18]2[O:19][C:20]3[CH:26]=[C:25]([O:27][CH3:28])[CH:24]=[CH:23][C:21]=3[N:22]=2)=[CH:16][N:17]=1

Participants

3

Reactant 2

HCID 24780800HCID 24780800, compoundHCID 59203852HCID 59203852, compound

Product 1

HCID 24780802HCID 24780802, compound

Procedure

The title compound was synthesized from tert-butyl (2-fluoroethyl)[5-(6-methoxy-1,3-benzoxazol-2-yl)pyrimidin-2-yl]carbamate according to the procedure described for N-(2-fluoroethyl)-5-(6-methoxy-1,3-benzoxazol-2-yl)pyridin-2-amine to give 29.8 mg. MS m/z 289 (M+H).

Workup

  1. customto give 29.8 mg

Sources & evidence

ORD record
ord-ef957cca0e25462c8797dd916b3c6527
Source dataset
uspto-grants-2010_03
Patent number
US07670591B2

Reaction notes

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