HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → 3,7,12-Triformyloxycholanoic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Cholic Acid | HCID 221493 | — |
| Reactant | HCID 86628349 | HCID 86628349 | — |
| Product | 3,7,12-Triformyloxycholanoic acid chloride | HCID 87433271 | — |
Reaction Steps
By a standard technique using cholic acid and formalin, 3,7,12-triformyloxycholanoic acid was synthesized. It was then chlorinated using oxalyl chloride. The crude product thus obtained was used in the subsequent step of esterification without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07670751B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-51e728a84fe84d01ab2b2eb6a72be817 |
| Source note | uspto-grants-2010_03 |