Water → HCID 39733476, compound

HRID 2241850Notes

Reaction equation

HRID 2241850 reaction equation
C(O[C:4]([N:6]1[C:10](=[O:11])[C:9]2=[CH:12][CH:13]=[CH:14][CH:15]=[C:8]2[C:7]1=[O:16])=O)C.[OH2:17]>>[C:7]1(=[O:16])[N:6]([CH2:4][CH2:4][NH:6][CH2:7][CH2:8][OH:17])[C:10](=[O:11])[C:9]2=[CH:12][CH:13]=[CH:14][CH:15]=[C:8]12

Participants

3

Reactant 2

HCID 962WaterHCID 31187N-Carbethoxyphthalimide

Product 1

HCID 39733476HCID 39733476, compound

Procedure

10.4 g (0.1 mol) of N,N-(2-hydroxyethyl),ethyl amine and 22 g (0.1 mol) of N-ethoxycarbonyl phthalimide were dissolved in 50 ml of H2O and stirred for 2 hours. The reaction mixture was lyophilized and the solid product washed with methanol (40 ml). The remaining white solid (Compound 14) was collected and dried.

Workup

  1. washthe solid product washed with methanol (40 ml)
  2. customThe remaining white solid (Compound 14) was collected
  3. customdried

Sources & evidence

ORD record
ord-a0833a772ec54d8f82d52cb4a3c01c0b
Source dataset
uspto-grants-2010_03
Patent number
US07671036B2

Reaction notes

Loading…