HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Hexyloxybenzyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-(Chloromethyl)-4-Ethoxybenzene | HCID 2063971 | — |
| Reactant | [4-(Hexyloxy)phenyl]methanol | HCID 3895948 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-Hexyloxybenzyl Chloride | HCID 10376434 | — |
Reaction Steps
This molecule was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (7.17 g, 60.3 mmol), 4-hexyloxybenzyl alcohol (11.3 g, 54.3 mmol), CH2Cl2 (150 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07671033B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-73663425d1c5459c94f29258d3cba0d7 |
| Source note | uspto-grants-2010_03 |