Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-Decyloxybenzyl Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 1-(Chloromethyl)-4-(dodecyloxy)benzene | HCID 10086755 | — |
| 반응물 | 4-Decyloxybenzyl alcohol | HCID 13079652 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-Decyloxybenzyl Chloride | HCID 20149012 | — |
반응 단계
Was synthesized following the same general procedure as that for the preparation of 4-dodecyloxybenzyl chloride; thionyl chloride (5.00 g, 42.4 mmol), 4-decyloxybenzyl alcohol (10.2 g, 38.6 mmol), CH2Cl2 (100 mL). 9.87 g (90%) white solid which decomposes upon melting.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07671033B2 |
| 출처 데이터셋 | uspto-grants-2010_03 |
| ORD ID | ord-a033880df3c848cfbf8807a3cf38d580 |
| 출처 메모 | uspto-grants-2010_03 |