HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Tetradecyloxybenzyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-(Chloromethyl)-4-(dodecyloxy)benzene | HCID 10086755 | — |
| Reactant | 4-Tetradecyloxybenzyl alcohol | HCID 10087384 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-Tetradecyloxybenzyl Chloride | HCID 20383169 | — |
Reaction Steps
This one was synthesized following the same general procedure as that for the preparation of 4-dodecyloxybenzyl chloride; thionyl chloride (7.45 g, 63.1 mmol), 4-tetradecyloxybenzyl alcohol (18.4 g, 57.4 mmol), CH2Cl2 (150 mL). 16.28 g (84%) white solid which decomposes upon melting.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07671033B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-491d7b64a93142079ff53b56ef5f3e85 |
| Source note | uspto-grants-2010_03 |