Veratroyl chloride → 3-benzyloxy-benzoic acid (Z)-2-(3,5-dichloro-pyridin-4-yl)-1-(3,4-dimethoxy-phenyl)vinyl ester

HRID 2242076Notes

Reaction equation

HRID 2242076 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6](Cl)=[O:7].[Cl:14][C:15]1[CH:16]=[N:17][CH:18]=[C:19]([Cl:22])[C:20]=1[CH3:21].[CH2:23]([O:30][C:31]1[CH:32]=[C:33]([CH:37]=[CH:38][CH:39]=1)[C:34](Cl)=[O:35])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[Cl:14][C:15]1[CH:16]=[N:17][CH:18]=[C:19]([Cl:22])[C:20]=1/[CH:21]=[C:6](\[O:7][C:34](=[O:35])[C:33]1[CH:37]=[CH:38][CH:39]=[C:31]([O:30][CH2:23][C:24]2[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=2)[CH:32]=1)/[C:5]1[CH:9]=[CH:10][C:11]([O:12][CH3:13])=[C:3]([O:2][CH3:1])[CH:4]=1

Participants

4

Reactant 3

HCID 77070Veratroyl chlorideHCID 49953753-Benzyloxybenzoyl chlorideHCID 109538273,5-Dichloro-4-methylpyridine

Product 1

HCID 248258303-benzyloxy-benzoic acid (Z)-2-(3,5-dichloro-pyridin-4-yl)-1-(3,4-dimethoxy-phenyl)vinyl ester

Procedure

The compound was obtained starting from 3,4-dimethoxy-benzoyl chloride, 3,5-dichloro-4-methylpyridine and 3-benzyloxy-benzoyl chloride, following the procedure of Example 24.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-18254009e1144bc4b0c96cb98bd96877
Source dataset
uspto-grants-2010_03
Patent number
US07671066B2

Reaction notes

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