HCID 68433578, compound → HCID 68430640, compound

Participants

Reaction Steps

To a solution of the material prepared in Step A (2.8 g, 6.1 mmol) in acetic acid (100 mL) was added solid platinum(IV) oxide (0.75 g). The mixture was placed under 3 atm of hydrogen gas at ambient temperature for 36 h. The mixture was filtered through Celite, and the resulting solution was concentrated in vacuo affording the title compound as a 2:1 mixture of cis and trans cyclohexyl diastereomers, which was used without further purification.

Provenance & Evidence