3,4-Difluoroaniline → HCID 11858754, compound

HRID 2242805Notes

Reaction equation

HRID 2242805 reaction equation
[N+:1](=[C:3]1[C:8](=[O:9])[CH2:7][CH2:6][CH2:5][C:4]1=[O:10])=[N-].[F:11][C:12]1[CH:13]=[C:14]([CH:16]=[CH:17][C:18]=1[F:19])N>>[F:11][C:12]1[CH:13]=[C:14]([N:1]([C:3]2[C:8](=[O:9])[CH2:7][CH2:6][CH2:5][C:4]=2[OH:10])[C:3]2[C:8](=[O:9])[CH2:7][CH2:6][CH2:5][C:4]=2[OH:10])[CH:16]=[CH:17][C:18]=1[F:19]

Participants

3

Reactant 2

HCID 774693,4-DifluoroanilineHCID 110624492-diazocyclohexane-1,3-dione

Product 1

HCID 11858754HCID 11858754, compound

Procedure

Following the procedure described in the Example 1, using 2-diazo-cyclohexane-1,3-dione and 3,4-difluoroaniline as starting materials to yield the title compound as a white solid.

Sources & evidence

ORD record
ord-a544e0ecac914788acaed775688392f2
Source dataset
uspto-grants-2010_03
Patent number
US07674793B2

Reaction notes

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