HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorobenzoic acid → HCID 23085749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorobenzoic acid | HCID 9935 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | 4-Nitro-1,2-phenylenediamine | HCID 5111791 | — |
| Solvent | Toluene ethylacetate | HCID 21584019 | — |
| Product | HCID 23085749 | HCID 23085749 | 15% |
Reaction Steps
Prepared from 4-nitrophenylenediamine and 2-fluorobenzoic acid, in a manner similar to that of Example 31b. Yield: 15%; Rf (7/3 toluene/ethyl acetate): 0.55; IR (KBr): 2996, 1625, 1520, 1479, 1340 cm−1; 1H-NMR (d6-DMSO) 8.5-8.0 (m, 3H); 7.2-7.9 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07674809B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-03df7ff84f9c468785517af7abe982f4 |
| Source note | uspto-grants-2010_03 |