Sulfuryl chloride → HCID 11177293, compound

HRID 2243154Notes

Reaction equation

[C:1]1([N:7]2[CH:11]=[CH:10][CH:9]=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:12]([C:14]1[CH:19]=[CH:18][C:17]([S:20](Cl)(=[O:22])=[O:21])=[CH:16][CH:15]=1)#[N:13].S(Cl)(Cl)(=O)=O>>[C:12]([C:14]1[CH:19]=[CH:18][C:17]([S:20]([NH:13][CH:12]([C:11]2[N:7]([C:1]3[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=3)[N:8]=[CH:9][CH:10]=2)[CH:14]([CH2:19][CH3:18])[CH2:15][CH3:16])(=[O:22])=[O:21])=[CH:16][CH:15]=1)#[N:13]

Participants

Reactant 3

HCID 24648Sulfuryl chloride

HCID 394974-Cyanobenzenesulfonyl chloride

HCID 707691-Phenylpyrazole

Product 1

HCID 11177293HCID 11177293, compound

Procedure

This compound was prepared using the method described in example 10, but 1-phenyl-1H-pyrazole was used as the starting material in step 10B and 4-cyanobenzenesulfonyl chloride was used as the sulfonyl chloride in step 10E. mp 134.6-136.6° C.; Mass Spectrum (−ES): 407.1 (M−H)−.

Workup

customThis compound was prepared

Sources & evidence

ORD record: ord-31565dd7b82c4c97a0e4fd70d1e317fa
Source dataset: uspto-grants-2010_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07674813B2

Reaction notes

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