HCID 68693110, compound → HCID 68694379, compound

Participants

Reaction Steps

A mixture of 8c (200 mg, 0.303 mmol, 1.0 equiv) and 10% Pd on carbon (30 mg) in EtOAc at 25° C. was exposed to a hydrogen atmosphere (balloon). Upon consumption of the starting material as indicated by TCL, the mixture was filtered and solvent removed in vacuo. The resulting phenol 8b was advanced without further purification. MS (MH+) 540; Calculated 539.3 for C31H33N5O4.

Provenance & Evidence