4-Hydroxyisophthalaldehyde → 4-(6-Phenylhexyloxy)-1,3-benzenedicarboxaldehyde

HRID 22436Notes

Reaction equation

HRID 22436 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[O:9])=[CH:4][C:3]=1[CH:10]=[O:11].[C:12]1([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]Cl)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:12]1([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:1][C:2]2[CH:7]=[CH:6][C:5]([CH:8]=[O:9])=[CH:4][C:3]=2[CH:10]=[O:11])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 1651064-HydroxyisophthalaldehydeHCID 5224111-Chloro-6-phenylhexane

Product 1

HCID 199302544-(6-Phenylhexyloxy)-1,3-benzenedicarboxaldehyde

Procedure

4-(6-phenylhexyloxy)-1,3-benzenedicarboxaldehyde was prepared from 4-hydroxy-1,3-benzenedicarboxaldehyde and 6-phenylhexyl chloride using the method in Example 1 at a higher reaction temperature of 140° C.

Workup

  1. customat a higher reaction temperature of 140° C.

Sources & evidence

ORD record
ord-4fad1b86f9eb46cc876c3d88934cb80b
Source dataset
uspto-grants-1995_06
Patent number
US05428065

Reaction notes

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