HRID224362

反应详情

EQUATION

反应方程式

HRID 224362 的结构方程式

PROCEDURE

实验过程

Using the procedure of Example 1, a mixture of 0.8 g of 5-nitro-1H-indole, 1.53 g of the hydrate of 4-piperidone hydrochloride and 16 ml of 2 N methanolic potassium hydroxide was reacted to obtain 0.86 g of raw product which was crystallized from isopropanol to obtain 0.74 g of 5-nitro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole melting at 250° C.

WORKUP

后处理

  1. customwas reacted
  2. customto obtain 0.86 g of raw product which
  3. customwas crystallized from isopropanol