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HRID224380

反应详情

EQUATION

反应方程式

HRID 224380 的结构方程式

REACTANTS

反应物

3
结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：CN(SSC1CCCCC1)C(=O)F
HCID22748626

未命名化合物

结构：CN1C(=O)C(C)(C)SC1=NO
HCID71363389

2-(Hydroxyimino)-3,5,5-trimethyl-1,3-thiazolidin-4-one

C6H10N2O2S

PRODUCTS

生成物

1
结构：CN(SSC1CCCCC1)C(=O)ON=C1SC(C)(C)C(=O)N1C
HCID53786550

未命名化合物

PROCEDURE

实验过程

2-[[O-[N-Methyl-N-(cyclohexylthiosulfenyl)carbamoyl]oximino]]-3,5,5-trimethylthiazolidin-4-one was prepared according to the procedure described in Example X by reacting 3.48 g (0.02 m) of 3,5,5-trimethyl-2-oximino thiazolidin-4-one with 4.47 g (0.02 m) of N-methyl-N-(cyclohexylthiosulfenyl) carbamoyl fluoride and 1.32 g (0.02 m) of potassium hydroxide. Weight of 2-[[O-[N-methyl-N-(cyclohexylthiosulfenyl)carbamoyl]oximino]]-3,5,5-trimethylthiazolidin-4-one produced was 3.1 g. m.p. 86°-88° C.

WORKUP

后处理

  1. custom2-[[O-[N-Methyl-N-(cyclohexylthiosulfenyl)carbamoyl]oximino]]-3,5,5-trimethylthiazolidin-4-one was prepared