HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 3-(2-(Trifluoromethoxy)phenyl)-5,6,7,8-tetrahydro-5,8-methanocinnoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo(2.2.1)heptane-2,3-dione | HCID 138696 | — |
| Reactant | [2-Oxo-2-(2-trifluoromethoxy-phenyl)-ethyl]-phosphonic acid dimethyl ester | HCID 86609928 | — |
| Product | 3-(2-(Trifluoromethoxy)phenyl)-5,6,7,8-tetrahydro-5,8-methanocinnoline | HCID 67363297 | — |
Reaction Steps
yellow gum. MS (EI): 306.2 (M+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, [2-Oxo-2-(2-trifluoromethoxy-phenyl)-ethyl]-phosphonic acid dimethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678795B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-050dfa46e14b4850814f678bc50629e9 |
| Source note | uspto-grants-2010_03 |