HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 23332913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2,4-Bis(trichloromethyl)-2H,4H-1,3-benzodioxine-6-sulfonyl chloride | HCID 23332966 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23332913 | HCID 23332913 | — |
Reaction Steps
Diethylamine (0.8 g.) was added dropwise to a stirred suspension of 2,4-bis(trichloromethyl)benzo[1,3]dioxin-6-sulphonyl chloride (4.7 g.) in absolute ethanol (20 ml.), the mixture was maintained under gentle reflux for 2 hours, and the resulting solution was allowed to cool slowly to give a crystalline product, which was recrystallised from aqueous methanol to give 6-diethylsulphamoyl-2,4-bis(trichloromethyl)benzo[1,3]dioxin, m.p. 125°-126° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232032 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-9135a77f0285445f92e484d3083d62fa |
| Source note | uspto-grants-1980_11 |