HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 86737315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | 2,4-Bis(trichloromethyl)-2H,4H-1,3-benzodioxine-6-carbaldehyde | HCID 23332922 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86737315 | HCID 86737315 | — |
Reaction Steps
A mixture of 2,4-bis(trichloromethyl)benzo[1,3]dioxin-6-carboxaldehyde (1.0 g.) and phenylhydrazine (0.27 g.) in chloroform (35 ml.) was heated under gentle reflux for 1 hour. The resulting solution was cooled and evaporated to dryness under reduced pressure, and the residue was crystallised from ethanol to give 6-phenylhydrazonomethyl-2,4-bis(trichloromethyl)benzo[1,3]dioxin, m.p. 203°-204° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232032 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-f5c714d07a2b41efabf93cd8a3870e8f |
| Source note | uspto-grants-1980_11 |