HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 3-Cyclobutyl-5,6,7,8-tetrahydro-5,8-methanocinnoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo(2.2.1)heptane-2,3-dione | HCID 138696 | — |
| Reactant | Dimethyl (2-cyclobutyl-2-oxoethyl)phosphonate | HCID 22768687 | — |
| Product | 3-Cyclobutyl-5,6,7,8-tetrahydro-5,8-methanocinnoline | HCID 67363304 | — |
Reaction Steps
light yellow solid. MS (ESI): 200.2 (M+). Prepared from bicyclo[2.2.1]heptane-2,3-dione, (2-Cyclobutyl-2-oxo-ethyl)-phosphonic acid dimethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678795B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-c237bb6404364423b81708be8003c15d |
| Source note | uspto-grants-2010_03 |