Acetyl chloride → HCID 23332945, compound

Participants

Reaction Steps

A mixture of 6,8-diamino-2,4-bis(trichloromethyl)benzo[1,3]dioxin (1 g.), acetic anhydride (25 ml.) and acetyl chloride (2 ml.) was heated on the steam bath for 10 hours. After cooling, the reaction mixture was evaporated to dryness under reduced pressure, and the residue was triturated with aqueous ethanol. The solid product thus obtained was crystallised from ethanol to give 6,8-bis(diacetylamino)-2,4-bis(trichloromethyl)benzo[1,3]dioxin, m.p. 182°-183° C.

Provenance & Evidence