HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 23332924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2,4-Bis(trichloromethyl)-2H,4H-1,3-benzodioxin-6-ol | HCID 23332944 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23332924 | HCID 23332924 | — |
Reaction Steps
A mixture of 6-hydroxy-2,4-bis(trichloromethyl)benzo[1,3]dioxin (1.0 g.) and acetic anhydride (10 ml.) was warmed on the steam bath for 15 minutes, and then cooled to ambient temperature. Water (40 ml.) was added, and the mixture stirred for 1 hour. The product was removed by filtration, washed with water, dried and crystallised from ethanol to give 6-acetoxy-2,4-bis(trichloromethyl)benzo[1,3]dioxin, m.p. 142°-144° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232032 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-47519d6e0b45497388cd692410609f1e |
| Source note | uspto-grants-1980_11 |