Carbon Dioxide → HCID 20535618, compound

HRID 224413Notes

Reaction equation

HRID 224413 reaction equation
[CH2:1]=[CH:2][CH:3]([NH:5][CH:6]=[O:7])[CH3:4].[CH2:8](OC(Cl)=O)[CH3:9].C(=O)=O>>[CH2:8]([O:7][CH:6]=[N:5][CH:3]([CH3:4])[CH:2]=[CH2:1])[CH3:9]

Participants

4

Reactant 3

HCID 280Carbon DioxideHCID 10928Ethyl chloroformateHCID 13521834HCID 13521834, compound

Product 1

HCID 20535618HCID 20535618, compound

Procedure

A mixture of 1.0 g. of N-(1-buten-3-yl)formamide and one equivalent of ethylchloroformate is stirred under N2 for 4 hours during which time CO2 is evolved. The solution is stirred under reduced pressure for 3 hours to remove any unreacted ethylchloroformate, and a residue of ethyl-N-(1-buten-3-yl)formimidate is obtained.

Workup

  1. additionA mixture of 1.0 g
  2. customto remove any unreacted ethylchloroformate

Sources & evidence

ORD record
ord-2f48d7f9eb114a2ea4a00eb8c2ca42f2
Source dataset
uspto-grants-1980_11
Patent number
US04232030

Reaction notes

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