HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 136183340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 57833557 | HCID 57833557 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 136183340 | HCID 136183340 | — |
Reaction Steps
The intermediate from Step 1 above is treated with BBr3 in methylene chloride at 0° C. for 12 h. After work-up and purification by a published procedure (J. F. W. McOmie and D. E. West, Org. Synth., Collect. Vol. V, 412 (1973)), the desired compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678804B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-45aa837308684bd9b5f1a11bdceba5e6 |
| Source note | uspto-grants-2010_03 |