HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 15952080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 15952274 | HCID 15952274 | — |
| Product | HCID 15952080 | HCID 15952080 | — |
Reaction Steps
The title compound was prepared from 10-[(2′-formyl-1,1′-biphenyl-4-yl)carbonyl]-N-(pyridin-3-ylmethyl)-10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-3-carboxamide of Example 56, Step B, and methylamine (8 M solution in ethanol) in the manner of Example 42, m.p. 149-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678787B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-395bf7ad85e7441682bd5178cf85d507 |
| Source note | uspto-grants-2010_03 |