HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thymol → HCID 23333158, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thymol | HCID 6989 | — |
| Reactant | 2,3-Dihydro-5-methyl-6-phenyl-benzofuran | HCID 12878338 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 23333158 | HCID 23333158 | — |
Reaction Steps
830 mg of 2,3-Dihydro-5-methyl-6-phenyl-benzofuran and 100 mg of palladium on charcoal are refluxed for 48 hours in 10 ml of freshly distilled p-cymol. After cooling, the mixture is filtered through talc and the filtrate evaporated. The residue is chromatographed on 15 g of Kieselgel. 5-Methyl-6-phenyl-benzofuran is eluted with toluene as a uniformly oily liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04232039 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-67a355f8859546deb5ea877ee89ccfc2 |
| Source note | uspto-grants-1980_11 |