HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Bromoethoxy)tetrahydro-2H-pyran → HCID 58826444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Bromoethoxy)tetrahydro-2H-pyran | HCID 86621 | — |
| Reactant | HCID 86611033 | HCID 86611033 | — |
| Product | HCID 58826444 | HCID 58826444 | — |
Reaction Steps
In analogy to example 11A (1R,3S,4S)-3-azido-4-hydroxy-cyclopentanecarboxylic acid methyl ester (CAS 213742-85-9) was reacted with 2-(2-bromoethoxy)tetrahydro-2H-pyran to give (3S,4S)-3-azido-4-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-cyclopentanecarboxylic acid methyl ester. Light yellow oil. MS 336.3 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07678917B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-a02ac8196d9e41af8229d1c72068ed18 |
| Source note | uspto-grants-2010_03 |