Acetic Acid → HCID 68693598, compound

Participants

Reaction Steps

To the thioimidate solution in MeOH (4 mL, 0.24 mmol) from Example 19, a pre-mixed piperidine (0.12 mL, 1.21 mmol) and HOAc (0.11 mL, 1.92 mmol) were added. The mixture was then stirred at room temperature overnight. After being concentrated in vacuo, the residue was purified by HPLC to give a white powder (21 mg). MS 496.1 and 498.1 (M+H, Cl pattern).

Provenance & Evidence