3-Chlorophenylacetic acid → 2-(3-chlorophenyl)acetyl Chloride

HRID 2245222Notes

Reaction equation

HRID 2245222 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH2:8][C:9]([OH:11])=O)[CH:5]=[CH:6][CH:7]=1.S(Cl)([Cl:14])=O>>[Cl:1][C:2]1[CH:3]=[C:4]([CH2:8][C:9]([Cl:14])=[O:11])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 158793-Chlorophenylacetic acidHCID 24386Thionyl Chloride

Product 1

HCID 106552492-(3-chlorophenyl)acetyl Chloride

Procedure

3-Chlorophenylacetic acid (19.7 g) in thionyl chloride (100 ml) was heated at reflux for 3 h.

Workup

  1. temperatureat reflux for 3 h.

Sources & evidence

ORD record
ord-7f6c0587fe67474c87359bb01b9dd901
Source dataset
uspto-grants-2010_03
Patent number
US07683058B2

Reaction notes

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