Benzylamine → HCID 86628107, compound

Participants

Reaction Steps

A mixture of aldehyde (0.56 g, 1.0 mmol) from Step L, benzylamine (0.15 mL, 1.4 mmol) and sodium triacetoxy borohydride (1.0 g, 4.7 mmol) in 50 mL dimethyl chloride was stirred at room temperature for 12 hr. The mixture was washed with sat. aq. NaHCO3, then brine, dried over MgSO4 and filtered. The solvent was evaporated under vacuum to give an oil (0.61 g), which was used in the next step without purification. MS: (MH)+ 624.5.

Provenance & Evidence