HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 59216600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86615029 | HCID 86615029 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59216600 | HCID 59216600 | — |
Reaction Steps
To a solution of 3-methoxy-1-methyl-5-nitroquinolinium 4-methylbenzenesulfonate in methanol is added sodium borohydride at room temperature. The mixture is stirred at room temperature for 2 h and water is added. Water is added and the mixture is extracted with ethyl acetate. The organic layer is dried, filtered and concentrated under reduced pressure to give 3-methoxy-1-methyl-5-nitro-1,2-dihydroquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07683076B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-bcd553b1c739468685437f237007afd3 |
| Source note | uspto-grants-2010_03 |