HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Sulfide → 1-Dodecanethiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Sulfide | HCID 402 | — |
| Reactant | 1-Dodecene | HCID 8183 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | 1-Dodecanethiol | HCID 8195 | — |
Reaction Steps
Under the conditions of Example 3, with an input of 38 liters per hour of hydrogen sulphide, 67.7 mmoles of dodecene-1 dissolved in diglyme at a concentration of 0.564 mole per liter were irradiated at 11° C. After 3 minutes of irradiation, 48.2 mmoles of n-dodecyl mercaptan were formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04233128 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-b779b01eec7b4804ae0da5ef95b9639e |
| Source note | uspto-grants-1980_11 |