(1,1'-Biphenyl)-4-sulphonyl chloride → HCID 16114082, compound

HRID 2245527Notes

Reaction equation

HRID 2245527 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH2:13][C:14]([NH:16][C@H:17]([C:22]([O:24]C)=[O:23])[CH2:18][CH:19]([CH3:21])[CH3:20])=[O:15])[CH:8]=[CH:7]2)([O-])=O.[C:26]1([C:36]2[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=2)[CH:31]=[CH:30][C:29]([S:32](Cl)(=[O:34])=[O:33])=[CH:28][CH:27]=1>>[C:26]1([C:36]2[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=2)[CH:31]=[CH:30][C:29]([S:32]([NH:1][C:4]2[CH:12]=[C:11]3[C:10](=[CH:6][CH:5]=2)[N:9]([CH2:13][C:14]([NH:16][C@H:17]([C:22]([OH:24])=[O:23])[CH2:18][CH:19]([CH3:21])[CH3:20])=[O:15])[CH:8]=[CH:7]3)(=[O:34])=[O:33])=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 74192(1,1'-Biphenyl)-4-sulphonyl chlorideHCID 68541310HCID 68541310, compound

Product 1

HCID 16114082HCID 16114082, compound

Procedure

The title compound was prepared from methyl N-[(5-nitro-1H-indol-1-yl)acetyl]-L-leucinate and biphenyl-4-sulfonyl chloride following the procedures of Example 10 Step 4 and Step 5: MS (ESI) m/z 520; MS (ESI) m/z 518.

Sources & evidence

ORD record
ord-b4422c8d4f4246699995127364ce3c54
Source dataset
uspto-grants-2010_03
Patent number
US07683091B2

Reaction notes

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