Diethyl Ether → HCID 86633511, compound

Participants

Reaction Steps

Diethanolamine (0.22 g) was dissolved in water (0.5 mL), and to this was added an ether solution (3 mL) containing propionylacetic acid (0.25 g). Next, the mixture was stirred at 15° C. while an aqueous solution (1 mL) containing silver nitrate (0.34 g) was added dropwise, and this was further stirred for 15 minutes. The white precipitate that settled was filtered off to obtain silver propionylacetate (yield 1.89 g). FIG. 3 shows the infrared absorption spectrum (IR) of the silver propionylacetate that was obtained. IR:1714 cm−1, 1505 cm−1.

Provenance & Evidence