HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 24805263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Trimethyl orthoformate | HCID 9005 | — |
| Reactant | 2-Methyl-2H-pyrazol-3-ylamine | HCID 136927 | — |
| Reactant | HCID 59216810 | HCID 59216810 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 24805263 | HCID 24805263 | — |
Reaction Steps
The title compound was prepared according to general Method B. using 4-Chloro-N-(5-chloro-2-hydrazinocarbonyl-pyridin-3-yl)-3-trifluoromethyl-benzenesulfonamide (100 mg, 0.234 mmol), trimethylorthoformate (80 mg, 0.75 mmol), acetonitrile (2 mL), 2-Methyl-2H-pyrazol-3-ylamine (48 mg, 0.50 mmol) and acetic acid (1.0 mL). MS (ES) [M+H]+ expected 518.0, found 518.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07683176B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-e2150bd8453e47d19813076b1050cf40 |
| Source note | uspto-grants-2010_03 |