Acetonitrile → HCID 24802949, compound

Participants

Reaction Steps

The title compound was prepared according to general Method B using 4-Chloro-N-(5-chloro-2-hydrazinocarbonyl-pyridin-3-yl)-3-trifluoromethyl-benzenesulfonamide (100 mg, 0.234 mmol), trimethylorthoformate (80 mg, 0.75 mmol), acetonitrile (2 mL), 2-methylaniline (62 mg, 0.50 mmol) and acetic acid (1.0 mL). 1H NMR: (CD3OD, ppm): 8.82 (s, 1H), 8.40 (s, 1H), 8.27 (d, 1H), 8.05 (m, 1H), 7.75 (d, 1H), 7.61 (s, 1H), 7.39 (m, 1H), 7.32 (m, 1H), 7.25 (m, 2H), 2.15 (s, 3H). MS (ES) [M+H]+ expected 528.0, found 528.0.

Provenance & Evidence