Hydroxylamine → 2-Chloro-N'-hydroxy-4-[(methylsulfonyl)amino]benzenecarboximidamide

Participants

Role	Name	HCID	Charge
Reactant	Hydroxylamine	HCID 787	—
Reactant	N-(3-chloro-4-cyanophenyl)methanesulfonamide	HCID 669685	—
Solvent	Ethanol	HCID 702	—
Product	2-Chloro-N'-hydroxy-4-[(methylsulfonyl)amino]benzenecarboximidamide	HCID 72533799	—

Reaction Conditions

Temperature	90 °C

Reaction Steps

To a stirred solution of the product from Step A (0.13 g, 0.565 mmol) in ethanol (3 mL) was added hydroxylamine (50% in water, 1.0 mL). The reaction was heated at 90° C. for 2 h. The reaction was then concentrated to give the desired product.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07687492B2
Source dataset	uspto-grants-2010_03
ORD ID	ord-29c660b8b31b4cfb89eb3c7c518f418c
Source note	uspto-grants-2010_03