HCID 68529891, compound → HCID 68529942, compound

Participants

Reaction Steps

To a solution of Compound 49 (25 mg) in dimethoxyethane (1 ml) and ethanol (1 ml) was added 10% palladium on charcoal (10 mg). The mixture was stirred under hydrogen balloon pressure for 16 hours at room temperature. The resulted mixture was filtrated through Celite and the solvents were removed by rotary evaporation. The residue was purified by prepared TLC plate, eluting with methanol/dichloromethane (50/50), to afford Compound 50 as a yellow solid.

Provenance & Evidence