HCID 68527042, compound → HCID 68527620, compound

Participants

Reaction Steps

A mixture of Compound 56 (180 mg, 0.25 mmol), 10% palladium on carbon (36 mg, 20%) in 6 mL of ethanol was hydrogenated for 18 hours at a balloon pressure of hydrogen at 21° C. The catalyst was removed by filtration over celite and the filtrate was evaporated to give a crude product, which was chromatographed to give the desired product.

Provenance & Evidence