HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68531620, compound → HCID 68528802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68531620 | HCID 68531620 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68528802 | HCID 68528802 | — |
Reaction Steps
A mixture of Compound 63 (70 mg, 0.1 mmol), 10% palladium on carbon (20 mg, 20%) in 20 mL of ethanol was hydrogenated for 18 hours at a balloon pressure of hydrogen at 21° C. The catalyst was removed by filtration over celite and the filtrate was evaporated to give a crude product, which was chromatographed to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687496B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-1f0afd9790934cedaf9d22b685e87370 |
| Source note | uspto-grants-2010_03 |