HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinecarbonyl chloride, hydrochloride (1:1) → HCID 23331763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 7271866 | HCID 7271866 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 23331763 | HCID 23331763 | 13.2% |
Reaction Steps
In 1,2-dichloroethane, 2-(2,5-dimethylpyrrol-1-yl)-ethyl methyl ether was reacted with nicotinoyl chloride hydrochloride in the presence of aluminum chloride. The reaction product was chromatographed on a column of silica gel using cyclohexane/ethyl acetate (1/1) as an eluent to afford compound (260) in a yield of 13.2%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04233309 |
| Source dataset | uspto-grants-1980_11 |
| ORD ID | ord-32b8d0ae24bb470ab03bab67fc189b1a |
| Source note | uspto-grants-1980_11 |