HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68696643, compound → HCID 68089227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68696643 | HCID 68696643 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68089227 | HCID 68089227 | 96.5% |
Reaction Steps
A suspension of 2-methyl-5-nitro-1H-indole-1-acetic acid, ethyl ester (6.2 g) in ethanol (600 ml) in the presence of 10% palladium on charcoal (0.6 g) was stirred under a hydrogen atmosphere at 3 bar for 4 hours. The mixture was filtered through celite and the filtrate evaporated to give the sub-title compound as a pink viscous oil (5.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687535B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-b74b9ac43da94188b28d56f826bd7160 |
| Source note | uspto-grants-2010_03 |