HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,4-Dichlorophenyl)boronic acid → HCID 59218654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,4-Dichlorophenyl)boronic acid | HCID 2734659 | — |
| Reactant | 6-Chloro-2-(methylamino)-3-nitrobenzonitrile | HCID 11218089 | — |
| Product | HCID 59218654 | HCID 59218654 | 19% |
Reaction Steps
The title compound was prepared in 19% yield from 2,4-dichloro-phenylboronic acid and 6-chloro-2-methylamino-3-nitro-benzonitrile according to the procedure for Example 1A. 1H NMR (400 MHz, CDCl3): δ 7.49 (s, 1H), 7.24-7.31 (m, 2H), 6.89 (d, 1H, J=8.4 Hz), 6.78 (d, 1H, J=8.0 Hz), 3.67 (br s, 3H), 2.97 (s, 3H). MS (ES) [m+H] calc'd for C14H11N3Cl2, 292, 294; found 292, 294.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687638B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-267a2d9fb0e948b0ad68a327aa2b743d |
| Source note | uspto-grants-2010_03 |