反应详情

The title compound was prepared in 59% yield from 2-methoxy-phenylboronic acid and 2-amino-6-chloro-3-nitro-benzonitrile according to the procedure outlined for Example 5A. 1H NMR (400 MHz, CDCl3): δ 8.36 (d, 1H, J=8.8 Hz), 7.42-7.48 (m, 1H), 7.24-7.28 (m, 1H), 7.01-7.10 (m, 2H), 6.82 (br s, 2H), 6.78 (d, 1H, J=8.8 Hz), 3.86 (s, 3H). MS (ES) [m+H] calc'd for C14H11N3O3, 270; found 270.