HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylpyrrolidine → HCID 68441427, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylpyrrolidine | HCID 3146743 | — |
| Reactant | HCID 68441607 | HCID 68441607 | — |
| Product | HCID 68441427 | HCID 68441427 | — |
Reaction Steps
According to general procedure D, 0.10 g of (2S,4R,5R)-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidine-1,2-dicarboxylic acid 1-benzyl ester (from example 3b) and 3-phenylpyrrolidine are reacted to afford the title compound as a colourless solid. Rf=0.15 (EtOAc-heptane 1:1); Rt=5.47.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07687495B2 |
| Source dataset | uspto-grants-2010_03 |
| ORD ID | ord-0910f2265e6447cca7ec75769b14f014 |
| Source note | uspto-grants-2010_03 |